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Beilstein J. Org. Chem. 2011, 7, 824–830, doi:10.3762/bjoc.7.94
Graphical Abstract
Scheme 1: One-pot hydrozirconation-reductive coupling of allene 2 and nitrile 7.
Scheme 2: Cyclization of allenylnitrile 18.
Figure 1: Coupling constant analysis of the Boc-protected aminopyran ring in 21.
Scheme 3: Proposed chelated transition state model.
Scheme 4: Conversion of homoallylic amines to β-amino acid derivatives.